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Extraction of red cabbage anthocyanins: optimization of the operation conditions of the column process BABT
Xavier,Marcelo Fonseca; Lopes,Toni Jefferson; Quadri,Mara Gabriela Novy; Quadri,Marintho Bastos.
The aim of this work was to extract anthocyanins from the red cabbage. Batch studies under several extraction conditions indicated that acetic acid in aqueous solution (10% V/V) was the best solvent, used in the proportion of 0.25 g of red cabbage mL-1. At this condition, column assays were carried out to evaluate the influence of the ionic force, pH, solvent flow rate, recirculated volume of red cabbage juice and the mass of red cabbage. Results showed that the pH, recirculation and mass of red cabbage had statistically significant effects, where the optimum operation conditions found for the process were pH 2.3, recirculation volume of the solvent 0.83 L and mass of red cabbage 50 g.
Tipo: Info:eu-repo/semantics/article Palavras-chave: Anthocyanins; Extraction; Red cabbage; Experimental design; Optimization.
Ano: 2008 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-89132008000100018
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Adsorption of natural dyes on clay fixed on polymers BABT
Lopes,Toni Jefferson; Gonçalves,Odinei Hess; Barros,Ricardo Barbosa; Capelli,Francine Carla Rodrigues; Machado,Ricardo Antonio Francisco; Quadri,Mara Gabriela Novy; Quadri,Marintho Bastos.
The main purpose of this work was to produce a pellet to minimize undesirable effects in fixed beds, such as colmatation, through clay fixation on the surface of polymeric particles. Preliminary experiments were carried out by heating the clay, namely Tonsil Terrana 580FF, in order to observe variations on its capacity to adsorb anthocyanins derived from red cabbage. Clays was fixed on five samples of high density polyethylene (HDPE) at 180°C -210°C for two hours. The morphological analyses of the resulting particles were accomplished through Scanning Electron Microscopy (SEM). The experiments demonstrated an increase on clay's adsorptive capacity of 15.65% at 120°C for 30 hours and 16.80% at 170°C for two hours. The SEM analysis showed that the clay...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Adsorption; Clay; Polymer; Anthocyanin/red cabbage.
Ano: 2005 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-89132005000400034
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Evaluation of red cabbage anthocyanins after partial purification on clay BABT
Lopes,Toni Jefferson; Yaginuma,Sandra Regina; Quadri,Mara Gabriela Novy; Quadri,Marintho Bastos.
The aim of this work was to evaluate the red cabbage anthocyanins quality after purification by static adsorption assays on clay (Tonsil Terrana 580FF). Thin-layer chromatography analysis and scan spectrometry on UV-Visible showed a good dye stability of the pigment interacting with the clay. The use of pH 3.0 buffer during the batch assays provided a protective effect on the cabbage anthocyanins, limiting the dye acid hydrolyses. Analyses of the reducing sugars contents of the extract showed that clay retained 20% average of total free sugars under the test conditions.
Tipo: Info:eu-repo/semantics/article Palavras-chave: Thin-layer chromatography; Spectrophotometry; Purification; Batch conditions.
Ano: 2011 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-89132011000600022
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