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Tipificación y caracterización de café comercial mediante métodos instrumentales y quimiometría. Colegio de Postgraduados
Vázquez Hernández, Lorena.
El control de calidad de los productos agroalimentarios está basado en su caracterización bioquímica, como una de las partes esenciales. Para el caso del café, la composición química está fuertemente relacionada con las condiciones agroecológicas (suelo, clima, altura, etc.) de cada una de las regiones productoras. El café es la segunda materia prima en importancia en el mercado nacional, por lo cual, la calidad es importante para este producto. Para asegurarnos de la calidad del café tanto para los consumidores como productores existe la necesidad de establecer métodos analíticos, rápidos, objetivos y sensitivos. Para realizar la caracterización del café comercial existen métodos convencionales establecidos en la Norma Mexicana (NMX-F-013-SCFI-2000),...
Palavras-chave: Café; Quimiometría; NIRS; Homogeneidad; PCA; SIMCA; Coffee; Chemometrics; Homogeneity; Maestría; Producción Agroalimentaria en el Trópico.
Ano: 2011 URL: http://hdl.handle.net/10521/561
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Tipificación y caracterización de café comercial mediante métodos instrumentales y quimiometría. Colegio de Postgraduados
Vázquez Hernández, Lorena.
El control de calidad de los productos agroalimentarios está basado en su caracterización bioquímica, como una de las partes esenciales. Para el caso del café, la composición química está fuertemente relacionada con las condiciones agroecológicas (suelo, clima, altura, etc.) de cada una de las regiones productoras. El café es la segunda materia prima en importancia en el mercado nacional, por lo cual, la calidad es importante para este producto. Para asegurarnos de la calidad del café tanto para los consumidores como productores existe la necesidad de establecer métodos analíticos, rápidos, objetivos y sensitivos. Para realizar la caracterización del café comercial existen métodos convencionales establecidos en la Norma Mexicana (NMX-F-013-SCFI-2000),...
Palavras-chave: Café; Quimiometría; NIRS; Homogeneidad; PCA; SIMCA; Coffee; Chemometrics; Homogeneity; Maestría; Producción Agroalimentaria en el Trópico.
Ano: 2011 URL: http://hdl.handle.net/10521/561
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High-resolution prediction of organic matter concentration with hyperspectral imaging on a sediment core ArchiMer
Jacq, Kévin; Perrette, Yves; Fanget, Bernard; Sabatier, Pierre; Coquin, Didier; Martinez-lamas, Ruth; Debret, Maxime; Arnaud, Fabien.
In the case of environmental samples, the use of a chemometrics-based prediction model is highly challenging because of the difficulty in experimentally creating a well-ranged reference sample set. In this study, we present a methodology using short wave infrared hyperspectral imaging to create a partial least squares regression model on a cored sediment sample. It was applied to a sediment core of the well-known Lake Bourget (Western Alps, France) to develop and validate a model for downcore high resolution LOI550 measurements used as a proxy of the organic matter. In lake and marine sediment, the organic matter content is widely used, for example, to reconstruct carbon flux variations through time. Organic matter analysis through routine analysis methods...
Tipo: Text Palavras-chave: Hyperspectral imaging; Chemometrics; Near-infrared spectroscopy; High resolution analysis; Organic matter.
Ano: 2019 URL: https://archimer.ifremer.fr/doc/00478/59018/61636.pdf
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Digital Soil Mapping of Soil Properties in the “Mar de Morros” Environment Using Spectral Data Rev. Bras. Ciênc. Solo
Campbell,Patrícia Morais da Matta; Fernandes Filho,Elpídio Inácio; Francelino,Márcio Rocha; Demattê,José Alexandre Melo; Pereira,Marcos Gervasio; and,Clécia Cristina Barbosa Guimarães; Pinto,Luiz Alberto da Silva Rodrigues.
ABSTRACT Quantification of soil properties is essential for better understanding of the environment and better soil management. The conventional techniques of laboratory analysis are sometimes costly and detrimental to the environment. Thus, development of new techniques for soil analysis that do not generate residues, such as spectroscopy, is increasingly necessary as a viable way to estimate a wide range of soil properties. The objective of this study was to predict the levels of organic carbon (OC), clay, and extractable phosphorus (P), from the spectral responses of soil samples in the visible and near infrared (Vis-NIR), medium infrared (MIR), and Vis-NIR-MIR using different preprocessing methods combined with five prediction models. Soil samples were...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Spectral analysis; Reflectance; Chemometrics.
Ano: 2018 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-06832018000100314
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Soil Chemical and Spectroscopy Characteristics and the Effect of Management Practices Sci. Agrar.Paran. / SAP
Nogueira, Barbara Arruda; Merlin, Nathalie; Santos, Poliana Macedo dos; Santos, José Alfredo Baptista dos; Saab, Sergio da Costa; Tonial, Larissa Macedo dos Santos.
The aim of this study was to evaluated the facility to apply spectroscopic analysis coupled with chemometrics analysis as a rapid method for soil analysis. Soil samples from different depths (0-10, 10-20 and 20-30 cm) and treatment sites (area of fallow land for 5 years, area of no-tillage for 10 years and native forest) were applied in this study. Soil chemical characterization based on the concentration of macro-, micronutrients and the level of the toxic element showed significant different among to the samples under differences management systems. PCA and HCA analysis evaluated with soil chemical characterization showed that the samples were grouped according to the management systems. Similar results were obtained in the PCA and HCA analysis developed...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Spectroscopy; Chemometrics; Soil management; PCA; HCA.
Ano: 2018 URL: http://e-revista.unioeste.br/index.php/scientiaagraria/article/view/16175
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Grapevine leaf water potential based upon near infrared spectroscopy Scientia Agricola
Santos,Antonio Odair; Kaye,Oren.
Leaf water potential is a measure commonly used to describe crop water status and water stress dynamics. The established method for determining leaf water potential using a pressure chamber is cumbersome and subject to operator error as well as time/temperature limitations. These limitations prohibit the intensive sampling required to support proactive water management of commercial crops, including vineyards. Particular for grapevines there is need for faster, more precise and more reliable tools for determining leaf water potential in the field. Portable Near-infrared spectroscopy and multivariate data analysis were applied for the modeling and prediction of leaf water potential in grapevines. For field-grown wine grapes the most significant and...
Tipo: Info:eu-repo/semantics/article Palavras-chave: PLS; Irrigation; Spectrometry; Chemometrics.
Ano: 2009 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-90162009000300001
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Near-Infrared Spectroscopy for Non-Destructive Prediction of Maturity and Eating Quality of ‘Carabao’ Mango (Mangifera indica L.) Fruit CIGR Journal
Polinar, Yvonne Q.; Yaptenco, Kevin Fernandez; Peralta, Engelbert K.; Agravante, Josephine U..
Near-infrared (NIR) spectroscopy was assessed in predicting maturity and eating quality of ‘Carabao’ mango fruit. A total of 1,200 fruits were harvested at the green stage at four different harvest dates [100, 110, 120 and 125 days after flower induction (DAFI)]. Fruits were scanned at the green and table-ripe stage (TRS) using NIR reflectance spectroscopy. The fruits were then measured destructively for the determination of dry matter (DM) content at the green stage, total soluble solids (TSS) and sensory attributes at the TRS. The best calibration models were achieved using partial least square regression (PLSR) analysis for predicting DM, TSS and maturity in the short wavelength region of 700 - 990 nm at 2-nm increment. Principal component...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Agricultural / biosystems engineering; Chemometrics; Horticulture Near-infrared; Mango; Sweetness; Maturity; Eating quality; Philippines.
Ano: 2019 URL: http://www.cigrjournal.org/index.php/Ejounral/article/view/5152
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Green method by diffuse reflectance infrared spectroscopy and spectral region selection for the quantification of sulphamethoxazole and trimethoprim in pharmaceutical formulations Anais da ABC (AABC)
Silva,Fabiana E.B. da; Flores,Érico M.M.; Parisotto,Graciele; Müller,Edson I.; Ferrão,Marco F..
An alternative method for the quantification of sulphametoxazole (SMZ) and trimethoprim (TMP) using diffuse reflectance infrared Fourier-transform spectroscopy (DRIFTS) and partial least square regression (PLS) was developed. Interval Partial Least Square (iPLS) and Synergy Partial Least Square (siPLS) were applied to select a spectral range that provided the lowest prediction error in comparison to the full-spectrum model. Fifteen commercial tablet formulations and forty-nine synthetic samples were used. The ranges of concentration considered were 400 to 900 mg g-1SMZ and 80 to 240 mg g-1 TMP. Spectral data were recorded between 600 and 4000 cm-1 with a 4 cm-1 resolution by Diffuse Reflectance Infrared Fourier Transform Spectroscopy (DRIFTS). The proposed...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Chemometrics; Diffuse reflectance infrared Fourier transform spectroscopy; Green analytical method; High performance liquid chromatography; Interval partial least squares (iPLS); Synergy partial least squares (siPLS).
Ano: 2016 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0001-37652016000100001
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Best conditions for biodegradation of diesel oil by chemometric tools BJM
Kaczorek,Ewa; Bielicka-Daszkiewicz,Katarzyna; Héberger,Károly; Kemény,Sándor; Olszanowski,Andrzej; Voelkel,Adam.
Diesel oil biodegradation by different bacteria-yeast-rhamnolipids consortia was tested. Chromatographic analysis of post-biodegradation residue was completed with chemometric tools (ANOVA, and a novel ranking procedure based on the sum of ranking differences). These tools were used in the selection of the most effective systems. The best results of aliphatic fractions of diesel oil biodegradation were observed for a yeast consortia with Aeromonas hydrophila KR4. For these systems the positive effect of rhamnolipids on hydrocarbon biodegradation was observed. However, rhamnolipids addition did not always have a positive influence on the biodegradation process (e.g. in case of yeast consortia with Stenotrophomonas maltophila KR7). Moreover, particular...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Biodegradation; Chemometrics; Systems ranking; Variance analysis.
Ano: 2014 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1517-83822014000100017
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Chalcones and N-acylhydrazones: direct analogues? Exploratory data analysis applied to potential novel antileishmanial agents BJPS
Rando,Daniela Gonçalves; Giarolla,Jeanine; Pasqualoto,Kerly Fernanda Mesquita; Ferreira,Elizabeth Igne.
Leishmaniasis is an important health and social problem for which there is limited effective therapy. Chalcones and N-acylhydrazones have been studied as promising antileishmanial agents in enzymatic inhibition and in vitro assays. Since these chemical classes of compounds also resemble each other structurally, it would be useful to investigate whether they share direct analogy. Exploratory data analysis was applied to a library of chalcones and nitrated N-acylhydrazones assayed against Leishmania donovani to investigate their similarity. Under the conditions applied in the present study, the two classes did not present functional or structural analogy.
Tipo: Info:eu-repo/semantics/article Palavras-chave: Chalcones; N-acylhydrazones; Antileishmanial agents; Leishmaniasis; Chemometrics.
Ano: 2010 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1984-82502010000200019
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Assessment of physicochemical, textural and microbiological properties of brazilian white mold surface-ripened cheeses: a technological approach Ciência Rural
Pereira,Antonio Carlos Prestes; Judacewski,Priscila; Coelho,Gabriel; Salem,Renata Dinnies Santos; Marinho,Marina Tolentino; Alberti,Aline; Zielinski,Acácio Antonio Ferreira; Demiate,Ivo Mottin; Nogueira,Alessandro.
ABSTRACT: There are no specific technical regulations regarding the identity and quality of white mold surface-ripened cheeses in Brazil. These cheeses are sold both whole (Camembert-type) and in wedges (Brie-type). The aim of the study was to evaluate the physical and chemical properties; technological parameters and microbiological safety of 20 whole cheeses (Camembert-type) and 16 cheese wedges (Brie-type) produced in Brazil. Samples showed a wide range in sodium (91.0-731.0 mg/100 g, cheeses wedges) and calcium (238.0-1100.0 mg/100g, whole cheeses) contents. The cheese groups presented no significant differences in relation to the majority of the analyzed parameters. Listeria monocytogenes was reported in 5% of the whole cheese samples. The other...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Cheese quality; Chemometrics; Camembert-type cheese; Brie-type cheese.
Ano: 2020 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-84782020000100752
Registros recuperados: 11
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