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Determination of rare earth elements and other trace elements (Y, Mn, Co, Cr) in seawater using Tm addition and Mg(OH)(2) co-precipitation ArchiMer
Freslon, Nicolas; Bayon, Germain; Birot, Dominique; Bollinger, Claire; Barrat, Jean-alix.
This paper reports on a novel procedure for determining trace element abundances (REE and Y, Cr, Mn, Co) in seawater by inductively coupled plasma sector field mass spectrometry (ICP-SFMS). The procedure uses a combination of pre-concentration using co-precipitation onto magnesium hydroxides and addition of thulium spike. The validity of the method was assessed onto 25 ml volumes of certified reference materials (NASS- and CASS-4) and in house seawater standard. Procedural blanks were determined by applying the same procedure to aliquots of seawater previously depleted in trace elements by successive Mg(OH)(2) co-precipitations, yielding estimated contributions to the studied samples better than 1.1% for all elements, with the exception of Cr (<3.3%)...
Tipo: Text Palavras-chave: Trace elements; Rare earth elements (REE); Seawater; Mg(OH)(2) co-precipitation; ICP-MS; Thulium.
Ano: 2011 URL: http://archimer.ifremer.fr/doc/00041/15220/15855.pdf
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