Data/hora: 07/06/2024 08:00:06

Provedor de dados: | 52
País: | Brazil
Título: | Determination of trace metals in electrolytic copper by ICP OES and ICP-MS
Autores: | Santos,Éder José dos; Herrmann,Amanda Beatriz; Olkuszewski,José Luiz; Saint'Pierre,Tatiana D.; Curtius,Adilson José.
Data: | 2005-09-01
Ano: | 2005
Palavras-chave: | ICP-MS; Axial view ICP OES; Electrolytic copper; Electrodeposition.
Resumo: | The performance of axial view ICP OES and ICP-MS techniques were compared through the determination of As, Fe, Mn, Pb, Sb and Sn in electrolytic copper. Samples were prepared by two procedures: 1. Total dissolution with 5 % v/v HNO3 and 2. Dissolution with 1.4 % v/v HNO3 plus 2.0 % v/v H2SO4, followed by separation of the Cu by electrodeposition. The methods were applied for the analysis of standard copper solutions, using calibration against aqueous solutions with or without the addition of Cu. The results obtained by the two techniques were similar, but the separation of Cu from the sample matrix proved to be more adequate for practical reasons.
Tipo: | Info:eu-repo/semantics/article
Idioma: | Inglês
Identificador: | http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-89132005000600002
Editor: | Instituto de Tecnologia do Paraná - Tecpar
Relação: | 10.1590/S1516-89132005000600002
Formato: | text/html
Fonte: | Brazilian Archives of Biology and Technology  v.48 n.5 2005
Fonte: | info:eu-repo/semantics/openAccess