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Determinação potenciométrica em fluxo de cloreto de cetilpiridinio em desinfectantes bucais IPB - Escola Superior Agrária
Baptista, Paula; Araújo, Alberto N.; Montenegro, Maria da Conceição B. S. M..
The work describes a new procedure for cetylpyridinium chloride determination in oral disinfectants, based on a flow-injection system with potentiometric detection. The determination was based on the measurement of picrate concentration decrease as result of ion-pair reaction with the analyte present in the injected sample. In the optimised set-up the sample injection volume was kept at 400 µL and merged downstream with the reagent solution containing 1,0 x10-5 mol/L of picrate adjusted to pH 5.0 with citrate/citric acid buffer. The flow rate was fixed at 8 mL/min and the reactor length at 40 cm. The proposed procedure enables the determination of cetylpyridinium in the analytical range of 5,0x10-6 – 7,5x10-5 mol/L at a sampling rate of 60/h. The results...
Tipo: Article Palavras-chave: Potentiometry; Oral disinfectants; FIA; Ion-selective electrodes; Cationic surfactants; Spectrophotometric determination; Pharmaceutical preparations; Capillary electrophoresis; Pair extraction; Construction; Titrations; Sensor.
Ano: 2003 URL: http://hdl.handle.net/10198/938
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