Registro completo |
Provedor de dados: |
BJPS
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País: |
Brazil
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Título: |
Total polyphenols from Syzygium cumini (L.) Skeels fruit extract
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Autores: |
Migliato,Ketylin Fernanda
Carvalho,Elisângela Simões de
Sacramento,Luis Vitor Silva do
Mello,João Carlos Palazzo de
Baby,André Rolim
Velasco,Maria Valéria Robles
Salgado,Hérida Regina Nunes
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Data: |
2009-03-01
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Ano: |
2009
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Palavras-chave: |
Total polyphenols
Syzygium cumini
Botanical extract
Analytical method validation
Spectrophotometry
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Resumo: |
A precise, accurate and low cost spectrophotometric method was developed and validated for routine determination of total polyphenols, as pyrogallic acid equivalents, from the percolated and lyophilized extract of Syzygium cumini (L.) Skeels fruits. Validation was assessed experimentally and data were rigorously treated by statistical analysis. Analytical parameters were: linearity, interval (range), precision and recovery/accuracy, limit of detection (LOD, μg mL-1) and limit of quantification (LOQ, μg mL-1). The visible spectrophotometric method presented linearity (r² = 0.9979 ± 0.0010) over the concentration range 0.25-7.5 μg mL-1 of standard pyrogallic acid, precision < 2.918171%, recovery/accuracy ranging from 96.228693 to 107.17701%, LOD = 0.21 μg mL-1 and LOQ = 0.64 μg mL-1.
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Tipo: |
Info:eu-repo/semantics/article
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Idioma: |
Inglês
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Identificador: |
http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1984-82502009000100015
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Editor: |
Universidade de São Paulo, Faculdade de Ciências Farmacêuticas
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Relação: |
10.1590/S1984-82502009000100015
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Formato: |
text/html
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Fonte: |
Brazilian Journal of Pharmaceutical Sciences v.45 n.1 2009
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Direitos: |
info:eu-repo/semantics/openAccess
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