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| Registros recuperados: 40 | |
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| SILVA,Emily Marcele Soares; SILVA,Ingrid Reis da; OGUSKU,Mauricio Morishi; CARVALHO,Clarice Maia; MAKI,Cristina Sayuri; PROCÓPIO,Rudi Emerson de Lima. |
| ABSTRACT Tuberculosis (TB) remains one of the most deadly communicable infectious diseases, causing 1.4 million deaths in 2015 worldwide due to many conditions, including the inadequate treatment and the emergence of multidrug-resistant strains of the causal agent, Mycobacterium tuberculosis. Therefore, drugs developed from natural sources, as microorganisms and plant extracts, are a frequent target for the research and discovery of antimicrobial compounds. The current study started the characterization of compounds produced by an Aspergillus fumigatus isolated from copaíba (Copaifera multijuga) that efficiently inhibits M. tuberculosis by releasing the compounds into the fermentation broth under specific culture conditions. A preliminary assay was carried... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Mycobacterium spp.; Antimicrobial activity; Copaíba; Chromatography. |
| Ano: 2018 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0044-59672018000100063 |
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| J. SIMÃO,MARIELA; J.S. BARBOZA,THIAGO; G. VIANNA,MARCELA; GARCIA,RENATA; MANSUR,ELISABETH; P.R. IGNACIO,ANA CLAUDIA; PACHECO,GEORGIA. |
| Abstract Passiflora species are well known for their common use in popular medicine for the treatment of several diseases, such as insomnia, anxiety, and hysteria, in addition to their anti-inflammatory, antioxidant, analgesic and antibacterial potential. However, few data about the chemical composition and the medicinal potential of in vitro derived materials are available. Therefore, the goal of this work was to compare, for the first time, the phytoconstituents of in vitro derived materials of four Passiflora species, and evaluate the antibacterial potential of their extracts against 20 Gram-positive and negative strains. Chromatographic analysis indicated the presence of saponins in roots extracts from all studied species, whereas leaf extracts... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Antibacterial; Chromatography; Flavonoids; Passiflora; Saponins. |
| Ano: 2018 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0001-37652018000602805 |
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| Garcia,Edivaldo E; Kimura,Cláudia C.M; Martins,Ariovaldo C; Rocha,Gisele O; Nozaki,Jorge. |
| Gel permeation chromatography and high performance liquid chromatography were employed for separation and chemical characterization of products isolated from chrome shavings. After enzymatic hydrolysis, the products isolated were peptides of higher molecular weight. Peptides of lower molecular weight and free aminoacids were the main products using sulfuric acid in chrome shavings solubilization. Glycine (17%) , glutamic acid (10.6%) , alanine (9.2%) , and arginine (8.2%) were the principal amino acids found. Phenylalanine(1.8%) was the main aromatic amino acid , while tryptophane was completely absent. |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Chrome shavings; Enzyme; Chromatography; Protein; Chromium. |
| Ano: 1999 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-89131999000300003 |
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| Costa-Singh,Tainara; Jorge,Neuza. |
| Abstract The present study aims to evaluate the influence of extraction methods on the quality of bioactive compounds and antioxidant capacity in Pterodon emarginatusVogel (sucupira) oils. The oils were extracted from the sucupira seeds by Soxhlet and by the extraction system of Bligh & Dyer. The oils were analyzed as to fatty acid profile, tocopherols, phytosterols, carotenoids, total phenolics, and total antioxidant capacity. The extraction by Soxhlet showed better yield of total lipids and was more efficient to extract tocopherols, phytosterols, and carotenoids, besides presenting better antioxidant activity by DPPH•. However, this method showed insufficient capacity to extract the polar lipid components of the sample, as evidenced by the low... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Antioxidants; Bioactives; Extraction; Oxidative stability; Chromatography. |
| Ano: 2019 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-89132019000100506 |
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| Sher,Muhammad; Ahmad,Maria; Hassan,Faiza; Naeem-ul-Hassan,Muhammad; Hussain,Muhammad Ajaz. |
| A reverse phase high performance liquid chromatography method has been developed and validated for accelerated stability study and determination of pharmacokinetic parameters of venlafaxine HCl. The chromatographic separation was carried out using ODS analytical column (250 × 4.6 mm i.d., 5 µm particle size). The mobile phase included acetonitrile, methanol and potassium dihydrogen phosphate buffer (30:30:40; pH 6.1) at a flow rate 1.5 mL min−1. UV-Visible detector was used at wavelength of 227 nm to monitor elutions. Retention time observed was 2.745 min. The method was validated for linearity, accuracy, precision, sensitivity and robustness. Accelerated stability study of venlafaxine HCl capsules was carried out at 40 and 50 ºC under 75% RH level.... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Venlafaxine; HPLC; Stability; Pharmacokinetics; Chromatography. |
| Ano: 2020 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1984-82502020000100514 |
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| NAKANO,Viviane Emi; KUSSUMI,Tereza Atsuko; LEMES,Vera Regina Rossi; KIMURA,Iracema de Albuquerque; ROCHA,Sonia Bio; ALABURDA,Janete; OLIVEIRA,Maria Celeste Cardeal de; RIBEIRO,Reinaldo Amauri; FARIA,Ana Lúcia Rosa; WALDHELM,Kennia Cristian. |
| Pesticides in “PERA” orange samples (N = 57) from São Paulo City, Brazil were assessed and the pesticide intake contribution was estimated for chronic risk assessment. Seventy-six pesticides were evaluated by the gas chromatography multi-residue method, including isomers and metabolites (4.332 determinations). The mean recoveries at the limit of quantification level were in the range of 72-115% and the relative standard deviation for five replicate samples was 1-11%. The limits of detection and quantification ranged from 0.005 to 0.4 mg.kg−1 and from 0.01 to 0.8 mg.kg−1, respectively. Pesticides were found in 42.1% of the samples at levels ranging from 0.06 to 2.9 mg.kg−1. Of the contaminated samples, 3.5% contained residues (bifenthrin and clofentezine)... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Pesticide residues; Oranges; Public health; Risk assessment; Chromatography. |
| Ano: 2016 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0101-20612016000100040 |
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| Pacheco,Ariane Mendonça; Lucas,Ana; Parente,Rosana; Pacheco,Neuzimar. |
| Brazil nut has a high nutritional content and is a very important trade commodity to some Latin American countries. In order to evaluate its safety, 120 samples from different stages of the productive chain were analyzed in terms of: moisture content (mc), aflatoxigenic fungi and aflatoxin (LOQ = 1.95 μg.kg-1 total aflatoxin) using TLC. Among all samples, 4 (6.7%) from the receiving area, and 5 (16.7%), from retail presented aflatoxins above the LOQ, but the amount of aflatoxins was below the LOQ after the samples were dried in the plant. The positive samples were above the limit of total aflatoxin permitted by the European Union (4.0 μg.kg-1) and Brazil (30 μg.kg-1). The mc mean was 22.43% in the receiving area, which is higher than that in the other... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Bertholletia; Aspergillus; Moisture; Chromatography. |
| Ano: 2010 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0101-20612010000200007 |
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| OLIVEIRA,Rosane Gomes de; JAIN,Sona; LUNA,Alexandre Cândido; FREITAS,Lisiane dos Santos; ARAÚJO,Edilson Divino de. |
| Abstract Honey from stingless bees of the genus Melipona is a well sought product. Nevertheless lack of legal frameworks for quality assessment complicates the evaluation of food safety and marketing of these products. Seeking to assess the quality of honey from the bees of this genus, physical and chemical analyses, identification of phenolic compounds, and microbiological evaluation from six species of stingless bees was performed. The honey samples showed high reducing sugars, low protein levels and a balanced microbiota. High total phenols and flavonoids and higher antioxidant activity were also recorded. Different phenolic compounds of great biotechnological potential were identified and of these apigenin, kaempferol and luteolin were identified for... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Honey; Chromatography; Flavonoids; Phenols; Antioxidants; Stingless bees; Pollen types. |
| Ano: 2017 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0101-20612017000400552 |
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| Ferreira,Daniele de Freitas; Nora,Flávia Michelon Dalla; Lucas,Bruna Nichelle; Menezes,Cristiano Ragagnin de; Cichoski,Alexandre José; Giacomelli,Sandro Rogério; Wagner,Roger; Barin,Juliano Smanioto. |
| ABSTRACT: Essential oil extraction is commonly carried out by using the hydrodistillation method, which is described in official compendia of food quality control and medicinal plants. Despite the widespread use of this method, few studies have evaluated the effect of the atmosphere change during extraction on the composition and antioxidant activity of essentials oils. Therefore, a study of oxygen introduction influence during the extraction of essential oils from basil, lemongrass and lemon by hydrodistillation was performed. Total amount of oxygenated compounds (e.g., linalool, camphor, α-terpineol, neral, geranial, eugenol and α-muurolol) increased for all essential oils extracted under oxygen flow. Antioxidant activity evaluated by using the ORAC... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Antioxidant activity; Chromatography; ORAC; Volatile oil. |
| Ano: 2017 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-84782017000800752 |
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| Velázquez González, Julio César. |
| Dado que el picudo del chile es el principal problema fitosanitario en el cultivo de Capsicum spp., y las medidas de control no han logrado mitigar de forma eficiente las poblaciones de este insecto, se estudiaron los siguientes objetivos con el fin de conocer las interacciones planta insecto. Primero se valido un método de recolecta de volátiles, el cual demostró ser eficiente bajo las diferentes variables analíticas estudiadas, con % de recobro de 90-100 y DER menores a 10%. En segundo lugar se evaluó el potencial atrayente de estructuras de la planta como flores, yemas, frutos en desarrollo y frutos comerciales, encontrando que machos prefieren en primer lugar flores y después yemas, y las hembras en su primera opción eligieron yemas y después flores.... |
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Palavras-chave: Validación; Feromona; Capsicum; Sensilla; Cromatografía; Validation; Pheromone; Chromatography; Entomología y Acarología; Doctorado. |
| Ano: 2011 |
URL: http://hdl.handle.net/10521/557 |
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| Velázquez González, Julio César. |
| Dado que el picudo del chile es el principal problema fitosanitario en el cultivo de Capsicum spp., y las medidas de control no han logrado mitigar de forma eficiente las poblaciones de este insecto, se estudiaron los siguientes objetivos con el fin de conocer las interacciones planta insecto. Primero se valido un método de recolecta de volátiles, el cual demostró ser eficiente bajo las diferentes variables analíticas estudiadas, con % de recobro de 90-100 y DER menores a 10%. En segundo lugar se evaluó el potencial atrayente de estructuras de la planta como flores, yemas, frutos en desarrollo y frutos comerciales, encontrando que machos prefieren en primer lugar flores y después yemas, y las hembras en su primera opción eligieron yemas y después flores.... |
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Palavras-chave: Validación; Feromona; Capsicum; Sensilla; Cromatografía; Validation; Pheromone; Chromatography; Entomología y Acarología; Doctorado. |
| Ano: 2011 |
URL: http://hdl.handle.net/10521/557 |
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| Registros recuperados: 40 | |
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