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| Storck, Lindolfo; Departamento de Fitotecnia, Universidade Federal de Santa Maria, RS; Lúcio, Alessandro Dal’Col; Universidade Federal de Santa Maria; Krause, Willian; Universidade do Estado de Mato Grosso; Araújo, Dejânia Vieira de; Universidade do Estado de Mato Grosso; Silva, Celice Alexandre; Universidade do Estado de Mato Grosso. |
| There is a demand for research on yellow passion fruit plants (Passiflora edulis Sims) used for juice production. Thus, the present study aimed to determine the number of plants per experimental plot and the number of plots per genotype for different properties of passion fruit. The data used were obtained from an experiment (Tangará da Serra, Mato Grosso State, Brazil) that assessed 13 fruit properties in eight genotypes of yellow passion fruit plants, with 10 replicates and 10 plants per plot. For each of the 80 experimental plots, the optimum plot size (Xo) was estimated by the method of maximum curvature of the coefficient of variation model. The number of replicates for each genotype and the means were estimated through the use of 10 plants per plot,... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: 5.01.03.05-9 - melhoramento vegetal Passiflora edulis Sims; Yellow passion fruit; Experimental design; Accuracy Planejamento de experimentos. |
| Ano: 2014 |
URL: http://periodicos.uem.br/ojs/index.php/ActaSciAgron/article/view/17697 |
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| Fenilli,Tatiele A.B.; Reichart,Klaus; Bacchi,Osny O.S.; Trivelin,Paulo C.O.; Dourado-Neto,Durval. |
| The use of the 15N label for agronomic research involving nitrogen (N) cycling and the fate of fertilizer-N is well established, however, in the case of long term experimentation with perennial crops like citrus, coffee and rubber tree, there are still shortcomings mainly due to large plant size, sampling procedures, detection levels and interferences on the system. This report tries to contribute methodologically to the design and development of 15N labeled fertilizer experiments, using as an example a coffee crop fertilized with 15N labeled ammonium sulfate, which was followed for two years. The N of the plant derived from the fertilizer was studied in the different parts of the coffee plant in order to evaluate its distribution within the plant and the... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Experimental design; Replicate variability; Stable isotope methodology; Perennial crop. |
| Ano: 2007 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0001-37652007000400015 |
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| Cargnelutti Filho,Alberto; Alves,Bruna Mendonça; Follmann,Diego Nicolau; Bem,Cláudia Marques de; Schabarum,Denison Esequiel; Stefanelo,Lucas da Silva; Wartha,Cleiton Antonio; Kleinpaul,Jéssica Andiara; Chaves,Gabriela Görgen; Uliana,Daniela Barbieri; Pezzini,Rafael Vieira. |
| ABSTRACT The objectives of this work were to determine the optimum plot size and number of repetitions to evaluate the fresh matter weight of vetch (Vicia sativa L.) in sowing densities. Fortyeight uniformity trials of 6 m × 6 m were conducted. Sixteen trials were evaluated in each sowing density (40, 60, and 80 kg∙ha−1). Each trial was divided into 36 basic experimental units (BEU) of 1 m × 1 m, totaling 1,728 BEU. In each BEU, the fresh matter was weighed. The optimum plot size was determined by the method of maximum curvature of the coefficient of variation model. The means were compared among sowing densities by the Scott-Knott’s test. The number of repetitions — for experiments with completely randomized and randomized block designs, in scenarios of i... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Vicia sativa L.; Uniformity trials; Experimental design; Cover crops; Experimental precision. |
| Ano: 2017 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0006-87052017000200178 |
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| Lavezo,André; Cargnelutti Filho,Alberto; Bem,Cláudia Marques de; Burin,Cláudia; Kleinpaul,Jéssica Andiara; Pezzini,Rafael Vieira. |
| ABSTRACT The objectives of this study were to determine the optimum plot size (Xo) and the number of replications to evaluate grain yield and verify the variability of Xo among oat cultivars. Thirtytwo uniformity trials of 3 × 3 m were performed, being 8 from each cultivar (URS Charrua, URS Taura, URS Estampa, and URS Corona). Each uniformity trial was divided in 36 basic experimental units (BEU) of 0.5 × 0.5 m. Grain yield was determined in each BEU. The Xo was determined by the method of maximum curvature of the coefficient of variation model. Mean comparisons among cultivars were performed by the Scott-Knott test via bootstrap. The number of replications was calculated by an iterative process until convergence for experiments in completely randomized... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Avena sativa L.; Variability; Uniformity trial; Experimental design. |
| Ano: 2017 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0006-87052017000400512 |
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| Santos,Daniel; Lúcio,Alessandro Dal’Col; Cargnelutti Filho,Alberto; Lopes,Sidinei José; Olivoto,Tiago. |
| ABSTRACT The variability within rows of cultivation may reduce the accuracy of experiments conducted in a complete randomized block design if the rows are considered as blocks, however, little is known about this variability in protected environments. Thus, our aim was to study the variability of the fresh mass in lettuce shoot, growing in protected environment, and to verify the border effect and size of the experimental unit in minimizing the productive variability. Data from two uniformity trials carried out in a greenhouse in autumn and spring growing seasons were used. In the statistical analyses, it was considered the existence of parallel cultivation rows the lateral openings of the greenhouse and of columns perpendicular to these openings.... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Experimental accuracy; Experimental design; Experimental error; Lactuca sativa L.; Greenhouse. |
| Ano: 2018 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0006-87052018000200230 |
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| Cargnelutti Filho,Alberto; Lavezo,André; Bem,Cláudia Marques de; Carini,Fernanda; Schabarum,Denison Esequiel; Bandeira,Cirineu Tolfo; Kleinpaul,Jéssica Andiara; Wartha,Cleiton Antonio; Silveira,Daniela Lixinski; Pezzini,Rafael Vieira; Thomasi,Rosana Marzari; Simões,Fernanda Martins; Neu,Ismael Mario Márcio. |
| ABSTRACT The aim of this study was to determine the optimum plot size to evaluate the fresh matter of aerial part of dwarf pigeon pea (Cajanus cajan (L.) Millsp), cultivar IAPAR 43 (Aratã), in scenarios formed by combinations of numbers of treatments, number of replications, and precision levels. The fresh matter of aerial part was weighed on basic experimental units of 1 m × 1 m in three uniformity trials with size of 24 m × 12 m (288 m2 in each trial). The soil heterogeneity index of Smith was estimated. Also, the optimum plot size was determined by Hatheway’s method in scenarios formed by combinations of i treatments (i = 5, 10, 15, and 20), r replications (r = 3, 4, 5, 6, 7 8, 9, and 10), and d precision levels (d = 5%, 10%, 15%, 20%, 25%, and 30%). In... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Cajanus cajan L.; Fresh matter of aerial part; Uniformity trial; Experimental design; Cover crops. |
| Ano: 2018 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0006-87052018000200212 |
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| Xavier,Marcelo Fonseca; Lopes,Toni Jefferson; Quadri,Mara Gabriela Novy; Quadri,Marintho Bastos. |
| The aim of this work was to extract anthocyanins from the red cabbage. Batch studies under several extraction conditions indicated that acetic acid in aqueous solution (10% V/V) was the best solvent, used in the proportion of 0.25 g of red cabbage mL-1. At this condition, column assays were carried out to evaluate the influence of the ionic force, pH, solvent flow rate, recirculated volume of red cabbage juice and the mass of red cabbage. Results showed that the pH, recirculation and mass of red cabbage had statistically significant effects, where the optimum operation conditions found for the process were pH 2.3, recirculation volume of the solvent 0.83 L and mass of red cabbage 50 g. |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Anthocyanins; Extraction; Red cabbage; Experimental design; Optimization. |
| Ano: 2008 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-89132008000100018 |
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| Molin,Rochele Fernanda; Valduga,Alice Teresa; Di Luccio,Marco; Dartora,Nessana; Cichoski,Alexandre José; Pistore,Mônica; Rigo,Elisandra. |
| This work aimed to study the oxidation of leaves of Ilex paraguariensis St. Hil, in a process similar to the oxidation of Camellia sinensis, with the purpose of developing new products based on yerba maté. So far, no previous systematic study about the oxidation of yerba maté has been found elsewhere. A Plackett-Burman experimental design was used for the screening of the significant parameters that affected the oxidation. The oxidation was indirectly quantified by following the changes in the product color, water activity, and pH with the time of processing. The factors that most influenced the process were the age of the leaves and the relative humidity of the oxidation chamber. The differences between the treatments were more evident after 3, 6 12 and... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Physicochemical parameters; Yerba maté; Leave; Extract; Experimental design. |
| Ano: 2011 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-89132011000200016 |
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| Figueiredo,Vitória Ribeiro Garcia de; Justus,Ariana; Pereira,Dafne Garcia; Georgetti,Sandra Regina; Ida,Elza Iouko; Kurozawa,Louise Emy. |
| Abstract This work aimed to evaluate the enzymatic hydrolysis of okara protein concentrate with respect to degree of hydrolysis (DH) in order to obtain a protein hydrolysate with high antioxidant capacity and aglycones isoflavone content. A central composite rotatable design was carried out to evaluate the influence of temperature (40 to 70°C), enzyme:substrate ratio (0.5 to 5.0%, g/100g protein) and pH (7.0 to 9.0) on DH. The optimal condition was 55°C, pH 9 and enzyme:substrate ratio of 5.0%, resulting a DH value of 35.5%. After protein hydrolysis at optimal condition, the antioxidant capacities of hydrolysate increased from 58.29 to 383.49 μM Trolox equivalent/g solids (ABTS method) and 2.41 to 15.32 μM Trolox equivalent/g solids (FRAP method) when... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Soy pulp; Peptides; Cleavage of protein; Isoflavone profile; Electrophoresis; Experimental design. |
| Ano: 2019 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-89132019000100505 |
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| Vieira,Gabriela A.L.; Magrini,Mariana Juventina; Bonugli-Santos,Rafaella C.; Rodrigues,Marili V.N.; Sette,Lara D.. |
| ABSTRACT Pyrene and benzo[a]pyrene (BaP) are high molecular weight polycyclic aromatic hydrocarbons (PAHs) recalcitrant to microbial attack. Although studies related to the microbial degradation of PAHs have been carried out in the last decades, little is known about degradation of these environmental pollutants by fungi from marine origin. Therefore, this study aimed to select one PAHs degrader among three marine-derived basidiomycete fungi and to study its pyrene detoxification/degradation. Marasmiellus sp. CBMAI 1062 showed higher levels of pyrene and BaP degradation and was subjected to studies related to pyrene degradation optimization using experimental design, acute toxicity, organic carbon removal (TOC), and metabolite evaluation. The experimental... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Marine biotechnology; PAHs; Fungi; Acute toxicity; Experimental design. |
| Ano: 2018 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1517-83822018000400749 |
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| Smaniotto,Alessandra; Skovronski,Aline; Rigo,Elisandra; Tsai,Siu Mui; Durrer,Ademir; Foltran,Lillian Liva; Di Luccio,Marco; Oliveira,J. Vladimir; Oliveira,Débora de; Treichel,Helen. |
| The lipase produced by a newly isolate Sporidiobolus pararoseus strain has potential catalysis ability for esterification reactions. In order to improve its synthetic activity, this work aimed at optimizing 'synthetic lipase' production by submerged fermentation of a conventional media based on peptone, yeast extract, NaCl and olive oil using experimental design technique. According to the results obtained in the first experimental design (2(4-1)), yeast extract and NaCl concentrations were tested to further optimization by response surface methodology. The maximum 'synthetic lipase' activity obtained was 26.9 U/mL in the optimized media (5.0, 6.8, 7.0 and 1.0% (wt/v) of peptone, yeast extract, NaCl and olive oil, respectively), representing a 6.36-fold... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Sporidiobolus pararoseus; Experimental design; 'synthetic lipase'; Submerged fermentation. |
| Ano: 2012 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1517-83822012000400033 |
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| Corrêa,Juliana Moço; Christi,Divair; Torre,Carla Lieko Della; Henn,Caroline; Conceição-Silva,José Luis da; Kadowaki,Marina Kimiko; Simão,Rita de Cássia Garcia. |
| ABSTRACT A new strain of Thermomyces lanuginosus was isolated from the Atlantic Forest biome, and its β-xylosidases optimization in response to agro-industrial residues was performed. Using statistical approach as a strategy for optimization, the induction of β-xylosidases activity was evaluated in residual corn straw, and improved so that the optimum condition achieved high β-xylosidases activities 1003 U/mL. According our known, this study is the first to show so high levels of β-xylosidases activities induction. In addition, the application of an experimental design with this microorganism to induce β-xylosidases has not been reported until the present work. The optimal conditions for the crude enzyme extract were pH 5.5 and 60 °C showing better... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Experimental design; Saccharification; Β-Xylosidase; Thermomyces lanuginosus; Atlantic Forest. |
| Ano: 2016 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1517-83822016000300680 |
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| Ramos,Aline de Souza; Fiaux,Sorele Batista; Leite,Selma Gomes Ferreira. |
| Many Trichoderma species are able to produce 6-pentyl-α-pyrone (6-PP), a lactone with coconut-like aroma. In the present work, several culture parameters were studied to enhance the production of 6-PP by Trichoderma harzianum 4040 in solid-state fermentation. Green coir powder added to a nutrient solution was used as support material for fermentation. A Plackett-Burman screening technique was applied, followed by a fractionary factorial design. The best culture conditions within the experimental domain studied were (100 g support)-1: sucrose, 3 g; NaNO3, 0.24 g; (NH4)2SO4, 0.18 g; KH2PO4, 0.1 g; inoculum concentration, 2.2 x 10(6) spores; moisture level, 55%. The temperature established was 28ºC. The fermentation under the selected conditions led to a 6-PP... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: 6-pentyl-α-pyrone; Solid-state fermentation; Experimental design. |
| Ano: 2008 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1517-83822008000400022 |
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| Mercurio,Daiane Garcia; Calixto,Lívia Salomão; Campos,Patrícia Maria Berardo Gonçalves Maia. |
| Considering the importance of an adequate composition of the formulation in the development of stable, safe and effective cosmetic products, experimental design techniques are tools that can optimize the formulation development process. The objective of this study was to develop topical formulations using the Box-Behnken design with response surface methodology and evaluate its physical, sensory and moisturizing properties. The experimental design used in the first step allowed to identify and to quantify the influence of raw materials, as well as the interaction between them. In the second step, the analysis identified the influence of soy lecithin, the phytantriol and capric acid triglyceride and caprylic on the consistency index, stickiness and... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Emulsions; Formulation; Stability; Skin barrier; Experimental design. |
| Ano: 2020 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1984-82502020000100624 |
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| Papp,Lajos Attila; Gyéresi,Árpád; Hancu,Gabriel; Mircia,Eleonora; Kelemen,Hajnal. |
| A generic capillary zone electrophoresis method was developed for the analysis of four proton pump inhibitors: omeprazole, pantoprazole, lansoprazole and rabeprazole. During preliminary analysis screening of phosphate buffers at different pH levels was performed, in order to determine the optimum pH domain suitable for the simultaneous determination of all studied compounds. A face centered central composite design was employed for the optimization of separation conditions. The effect of buffer concentration, pH and applied voltage was studied; resolution between peaks and migration time of the last compound were considered as responses. Other factors as system temperature, injection parameters, capillary length, were held constant during the optimization... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Capillary electrophoresis; Proton-pump inhibitors; Experimental design. |
| Ano: 2019 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1984-82502019000100534 |
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| Cârcu-Dobrin,Melania; Sabău,Alexandra Georgiana; Hancu,Gabriel; Árpád,Gyéresi; Rusu,Aura; Kelemen,Hajnal; Papp,Lajos Attila; Cârje,Anca. |
| The present work describes the development of a capillary electrophoresis (CE) method for the chiral discrimination of amlodipine (AML) enantiomers using cyclodextrine (CD) derivatives as chiral selectors. A large number of native and derivatized, neutral and ionized CD derivatives were screened to find the optimal chiral selector; and carboximethyl-β-CD (CM-β-CD) was selected for the enantiomeric discrimination. A factorial analysis study was performed by orthogonal experimental design in which several factors were varied at the same time to optimize the separation method. The optimized method (25 mM phosphate buffer, pH = 9.0, 15 mM CM-β-CD, 15 ºC, + 25 kV, 30 mbar/1 second, detection wavelength 230 nm) was successfully applied for the baseline... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Amlodipine; Capillary electrophoresis; Chiral separation; Cyclodextrine; Experimental design. |
| Ano: 2020 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1984-82502020000100530 |
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| CAMPOS,Ana Paula Rocha; MATTIETTO,Rafaella de Andrade; CARVALHO,Ana Vânia. |
| Abstract Tucupi is a product obtained from the fermentation and cooking of cassava root wastewater which is widely used in the popular cuisine of the North region of Brazil. This study employed an experimental design to select tucupi processing (fermentation and cooking times) as a function of residual cyanidric acid content and assess the stability of the product obtained. Although the design did not generate a predictive mathematical model, the trend plots and physicochemical and sensory tests indicated 24 h of fermentation and 40 min of cooking as process parameters. The tucupi prepared had pH 3.71, titratable acidity of 0.7 g lactic acid/100 mL, 93.91% moisture, 0.5% ashes, 0.52% proteins, 0.24% lipids, 4.83% carbohydrates, total and free cyanide of... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Manihot esculeta; Cyanogenic compound; Experimental design; Sensory. |
| Ano: 2019 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0101-20612019000200365 |
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