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Preparation and characterization of alginate and gelatin microcapsules containing Lactobacillus rhamnosus Anais da ABC (AABC)
LOPES,SUSIANY; BUENO,LUCIANO; AGUIAR JÚNIOR,FRANCISCO DE; FINKLER,CHRISTINE.
ABSTRACT This paper describes the preparation and characterization of alginate beads coated with gelatin and containing Lactobacillus rhamnosus. Capsules were obtained by extrusion method using CaCl2 as cross linker. An experimental design was performed using alginate and gelatin concentrations as the variables investigated, while the response variable was the concentration of viable cells. Beads were characterized in terms of size, morphology, scanning electron microscopy (SEM), moisture content, Fourier Transform Infrared Spectrometry (FTIR), thermal behavior and cell viability during storage. The results showed that the highest concentration of viable cells (4.2 x 109 CFU/g) was obtained for 1 % w/v of alginate and 0.1 % w/v of gelatin. Capsules were...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Probiotics; Biopolymers; Functional foods; Microencapsulation.
Ano: 2017 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0001-37652017000401601
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Microencapsulation of a Colombian Spodoptera frugiperdaNucleopolyhedrovirus with Eudragit® S100 by spray drying BABT
Camacho Kurmen,Judith Elena; Gómez Alvarez,Martha Isabel; Villamizar Rivero,Laura Fernanda.
A Colombian Spodoptera frugiperda nucleopolyhedrovirus NPV003 with high potential for the development of an efficient biopesticide was microencapsulated by spray drying with a pH dependent polymer (Eudragit® S100). Conditions for microparticles production were standardized and microencapsulation process was validated. Physical properties, insecticide activity and photo-stability of microencapsulated virus were determined. The microparticles were spherical and irregular shaped, with sizes between 17.64 and 19.47 µm. Moisture content was 10.38 ± 0.87%; encapsulation efficiency 84.61± 13.09% and process yield was 91.20 ± 6.40%. Microencapsulation process did not affect viral insecticidal activity and provided efficient protection against UVB radiation....
Tipo: Info:eu-repo/semantics/article Palavras-chave: Baculovirus; Microencapsulation; Spray drying; Eudragit® S100; Photostability.
Ano: 2015 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-89132015000300468
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Characterization and shelf life of β-carotene loaded solid lipid microparticles produced with stearic acid and sunflower oil BABT
Gomes,Graziela Veiga de Lara; Borrin,Thais Ribeiro; Cardoso,Lisandro Pavie; Souto,Eliana; Pinho,Samantha Cristina de.
Solid lipid microparticles were tested as microencapsulation systems for protecting β-carotene from degradation. Blends of long-chain (C18) solid lipids (70% stearic acid) and sunflower oil (30%) were used to produce lipid microparticles encapsulating the carotenoid. Polysorbate 80 (4%) was employed to stabilize the stearic acid microparticles. The concentration of β-carotene was monitored using spectrophotometry, the particle size distribution was measured by laser diffraction, the crystal structure was determined by wide angle X-ray diffraction (WAXD), and the thermal behaviour was characterized by differential scanning calorimetry (DSC) over a period of seven months. All of the systems had an average particle size smaller than 5 µm. To avoid β-carotene...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Solid lipid microparticles; Β-carotene; Microencapsulation.
Ano: 2013 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-89132013000400017
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Poly-DL-lactide-co-glycolide microspheres as a controlled release antigen delivery system BJMBR
Lima,K.M.; Rodrigues Júnior,J.M..
Successful vaccine application means maximum protection with minimal number of administrations. A rational development of vaccines involves studies of the nature of the antigen as well as of the adjuvant to be used to improve the immune responses. This has provided the impetus for studies to design the degradable devices and for different approaches to antigen delivery by different routes of administration. The development of controlled release systems based on polymeric devices that permit a sustained or pulsed release of encapsulated antigens has attracted much interest. Polymeric delivery systems consist of polymers that release their content continuously in a controlled manner over a period of time. The development of a biocompatible delivery system...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Vaccine; Adjuvant; Microspheres; Microencapsulation; Biomaterial.
Ano: 1999 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-879X1999000200005
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Production and characterization of alginate-starch-chitosan microparticles containing stigmasterol through the external ionic gelation technique BJPS
Fujiwara,Gislene Mari; Campos,Ranieri; Costa,Camila Klocker; Dias,Josiane de Fátima Gaspari; Miguel,Obdulio Gomes; Miguel,Marilis Dallarmi; Marques,Francisco de Assis; Zanin,Sandra Maria Warumby.
Stigmasterol - a plant sterol with several pharmacological activities - is susceptible to oxidation when exposed to air, a process enhanced by heat and humidity. In this context, microencapsulation is a way of preventing oxidation, allowing stigmasterol to be incorporated into various pharmaceutical forms while increasing its absorption. Microparticles were obtained using a blend of polymers of sodium alginate, starch and chitosan as the coating material through a one-stage process using the external gelation technique. Resultant microparticles were spherical, averaging 1.4 mm in size. Encapsulation efficiency was 90.42% and method yield 94.87%. The amount of stigmasterol in the oil recovered from microparticles was 9.97 mg/g. This technique proved...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Stigmasterol/microencapsulation; Microencapsulation; Sodium alginate/drugs coating; Chitosan/drugs coating; Starch/drugs coating; Natural polymers/drugs coating.
Ano: 2013 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1984-82502013000300015
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Alginate-pomegranate peels' polyphenols beads: effects of formulation parameters on loading efficiency BJPS
Zam,Wissam; Bashour,Ghada; Abdelwahed,Wassim; Khayata,Warid.
Calcium alginate beads containing pomegranate peels' polyphenol extract were encapsulated by ionic gelation method. The effects of various formulation factors (sodium alginate concentration, calcium chloride concentration, calcium chloride exposure time, gelling bath time maintaining, and extract concentration) on the efficiency of extract loading were investigated. The formulation containing an extract of 1 g pomegranate peels in 100 mL distilled water encapsulated with 3 % of sodium alginate cured in 0.05 M calcium chloride for 20 minutes and kept in a gelling bath for 15 minutes was chosen as the best formula regarding the loading efficiency. These optimized conditions allowed the encapsulation of 43.90% of total extracted polyphenols and 46.34 % of...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Pomegranate/polyphenols/microencapsulation; Calcium alginate beads/microencapsulation; Microencapsulation; Polyphenols; Natural antioxidants/microencapsulation.
Ano: 2014 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1984-82502014000400741
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Effect of cellulose acetate phthalate and polyethylene glycol on physical properties and release of theophylline from microcapsules BJPS
Hussain,Amjad; Mumtaz,Ahmad Mehmood; Arshad,Muhammad Sohail; Abbas,Nasir; Latif,Abida; Shamim,Rahat; Bukhari,Nadeem Irfan; Hussain,Khalid.
ABSTRACT The present study describes the development of theophylline microcapsules by a non-solvent addition method and the effect of plasticizer addition on microencapsulation. The release was studied in distilled water and the data were analysed by various mathematical models for determining the mechanism of release. Prepared microcapsules were found to be spherical, free flowing and having more than 80% entrapped drug. The polymer - cellulose acetate phthalate and plasticizer - polyethylene glycol was considered to be affecting the properties of microcapsules including drug release (time for 50% drug release, T50). The formulation with the highest proportion of polymer and without plasticizer (F3) showed the slowest release with T50 = 4.3 h, while the...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Theophylline/microcapsules; Microencapsulation; Cellulose acetate phthalate; Polyethylene glycol; Microcapsules/mechanism of release; Drugs/release..
Ano: 2016 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1984-82502016000100004
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Characterization and evaluation of sensory acceptability of ice creams incorporated with beta-carotene encapsulated in solid lipid microparticles Ciênc. Tecnol. Aliment.
LIMA,Juliana Gobbi de; BRITO-OLIVEIRA,Thais Carvalho; PINHO,Samantha Cristina de.
Abstract The feasibility of incorporating beta-carotene-loaded solid lipid microparticles (BCSLM) into vanilla ice creams was investigated, through the physico-chemical characterization and evaluation of sensory acceptability of the products products. The BCSLM were produced with palm stearin as the lipid phase, hydrolyzed soy protein isolate as the surfactant, and xanthan gum as the thickener. The results showed similar values of proximate composition, total soluble solids, pH, and overrun for all formulations. On the other hand, colorimetric evaluations showed that the ice cream produced with partial substitution of artificial additives by BCSLM containing alpha-tocopherol presented a more intense color, while in the product with non-encapsulated...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Lipid particles; Ice cream; Palm stearin; Microencapsulation; Beta-carotene.
Ano: 2016 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0101-20612016000400664
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Microencapsulation of plum (Prunus salicina Lindl.) phenolics by spray drying technology and storage stability Ciênc. Tecnol. Aliment.
LI,Yibin; TANG,Baosha; CHEN,Junchen; LAI,Pufu.
Abstract To improve the stability of the phenolic extracts from plum fruit (Prunus salicina Lindl.), the microencapsulation conditions of spray drying were optimized by the response surface method. The Box-Behnken experimental results indicated the optimal conditions involved an inlet air temperature of 142.8 °C, a core material content of 23.7% and a feed solids content of 11.7%. The maximum microencapsulating efficiency was 87.7% at optimal conditions. Further, the physicochemical properties of the microcapsule powders were improved overall due to the addition of the coating agents. There were no statistically significant differences in phenolic content of the obtained microcapsules for the first 40 days of storage at 25 °C in dark condition (p >...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Prunus salicina Lindl.; Microencapsulation; Phenolics; Spray drying; Storage stability; Physicochemical properties.
Ano: 2018 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0101-20612018000300530
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Effects of storage conditions on phytochemical and stability of purple corn cob extract powder Ciênc. Tecnol. Aliment.
KAPCUM,Chutikarn; URIYAPONGSON,Juntanee.
Abstract Recently, purple corn cob has been gaining popularity for a dietary supplement and natural colorant. However, phytochemicals in waxy purple corn cob (WPC) are likely degraded during storage; thus, the microencapsulation by spray drying was used for lengthening those compounds. This work focused on the phenolic and anthocyanin content and antioxidant activity (AOA) in WPC extract microcapsules by hydroxypropyl beta-cyclodextrin (HPβCD) during storage at 4 and 30 °C for 60 days. The results revealed that only peonodin-3-glucoside at 30 °C was found as a higher decrease than 4 °C. Pelagonidin-3-glucoside and AOA were found more stable at both storage temperatures; however, the increase of protocatechuic acid and hydroxybenzoic acid were observed...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Waxy purple corn cob; Microencapsulation; Phenolics; Anthocyanins; Hydroxypropyl beta-cyclodextrin.
Ano: 2018 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0101-20612018000500301
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Evaluation of some residual bioactivities of microencapsulated Phaseolus lunatus protein fraction with carboxymethylated flamboyant (Delonix regia) gum/sodium alginate Ciênc. Tecnol. Aliment.
Sandovai-Peraza,Mukthar; Betancur-Ancona,David; Gallegos-Tintoré,Santiago; Chel-Guerrero,Luis.
Recent studies have shown the beneficial effect of peptides, an unexploited source could be Phaseolus lunatus being an important raw material for those functional products in order to improve their utilization. In addition to improve the beneficial effect of bioactive peptides the microencapsulation could be a way to protect the peptides against the environment to which they are exposed. P. lunatus protein fraction (<10 kDa of weight) was encapsulated using a blend of carboxymethylated flamboyant gum (CFG) and sodium alginate (SA) at different concentrations of CaCl2 and hardening times. After in vitro digestion of microcapsules the residual activity, in the intestinal system, both inhibition of agiotensin-converting enzyme (I-ACE) and antioxidant...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Microencapsulation; Flamboyant gum; Antioxidant activity; ACE-I activity.
Ano: 2014 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0101-20612014000400006
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Effect of added prebiotic (Isomalto-oligosaccharide) and Coating of Beads on the Survival of Microencapsulated Lactobacillus rhamnosus GG Ciênc. Tecnol. Aliment.
SIANG,Sing Chee; WAI,Lai Ka; LIN,Nyam Kar; PHING,Pui Liew.
Abstract The study aimed to encapsulate Lactobacillus rhamnosus GG (LGG) with the selected prebiotic, using co-extrusion technology with a poly-L-lysine (PLL) coating and evaluate probiotic survival in simulated gastrointestinal conditions. Selection of ideal prebiotic was conducted using inulin, fructo-oligosaccharide (FOS) and isomalto-oligosaccharide (IMO) and its optimal concentration to be incorporated in microencapsulation was determined. Microcapsules without coating (S1: no prebiotic and S3: with prebiotic) and with coating (S2: no prebiotic and S4: with prebiotic) produced were evaluated based on its physical properties and survival in simulated gastrointestinal environment. The IMO with a concentration of 3.0% (w/v) was selected due to its best...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Microencapsulation; Probiotic; Co-extrusion; Isomalto-oligosaccharide; Poly-L-lysine; Lactobacillus.
Ano: 2019 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0101-20612019000600601
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Microencapsulation of grape seed oil by spray drying Ciênc. Tecnol. Aliment.
BÖGER,Bruna Raquel; GEORGETTI,Sandra Regina; KUROZAWA,Louise Emy.
Abstract In the search for alternative wall materials to replace gum Arabic (GA), a good but expensive encapsulating agent, this work aimed to evaluate the effectiveness of maltodextrin 10DE in combination with GA (GA/MD, 50:50 ratio) for the microencapsulation of grape seed oil by spray drying. The addition of maltodextrin to gum Arabic did not influence the mean particle diameter, powder bulk density, encapsulation efficiency or the total oil retained in the microspheres. Although the oil encapsulated with GA showed greater retention of phenolic compounds after spray drying, the sample encapsulated with GA/MD had greater ferric reduction antioxidant power and DPPH radical scavenging activity, and a lower peroxide index.
Tipo: Info:eu-repo/semantics/article Palavras-chave: Microencapsulation; Grape seed oil; Antioxidant activity; Maltodextrin; Encapsulation efficiency; Lipid oxidation.
Ano: 2018 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0101-20612018000200263
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Retention of short chain fatty acids under drying and storage conditions Ciênc. Tecnol. Aliment.
Souza,Alexandre Santos; Rocha-Leão,Maria Helena; Borges,Soraia Vilela; Cirillo,Marcelo Ângelo; Cornejo,Félix Emílio Prado; Couri,Sônia.
Cheese whey permeate was used as a substrate for the fermentation of Propionibacterium freudenreichi PS1 for the production of short chain fatty acids, components of the bio-aroma of Swiss cheese. The liquid bio-aroma was encapsulated by spray drying under different conditions of air inlet temperature and feed rate. A study was carried out on the stability of the bio-aroma during storage in laminated packages at 30 °C for 96 days using the product showing the greatest retention of acetic and propionic acids. The results showed that the best drying conditions were an air entrance temperature of 180 °C and a feed rate of 24 g/min resulting in particles with a smooth surface and few invaginations and micro-fissures. However, 72% of the acetic acid and 80% of...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Fermentation; Microencapsulation; Spray drying; Swiss cheese flavor.
Ano: 2011 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0101-20612011000300039
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Microencapsulation: concepts, mechanisms, methods and some applications in food technology Ciência Rural
Silva,Pablo Teixeira da; Fries,Leadir Lucy Martins; Menezes,Cristiano Ragagnin de; Holkem,Augusto Tasch; Schwan,Carla Luisa; Wigmann,Évelin Francine; Bastos,Juliana de Oliveira; Silva,Cristiane de Bona da.
Microencapsulation is a process in which active substances are coated by extremely small capsules. It is a new technology that has been used in the cosmetics industry as well as in the pharmaceutical, agrochemical and food industries, being used in flavors, acids, oils, vitamins, microorganisms, among others. The success of this technology is due to the correct choice of the wall material, the core release form and the encapsulation method. Therefore, in this review, some relevant microencapsulation aspects, such as the capsule, wall material, core release forms, encapsulation methods and their use in food technology will be briefly discussed.
Tipo: Info:eu-repo/semantics/article Palavras-chave: Microcapsules; Microencapsulation; Controlled release.
Ano: 2014 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-84782014000701304
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Development, characterization and viability study of probiotic microcapsules produced by complex coacervation followed by freeze-drying Ciência Rural
Silva,Thaiane Marques da; Barin,Juliano Smanioto; Lopes,Eduardo Jacob; Cichoski,Alexandre José; Flores,Erico Marlon de Moraes; Silva,Cristiane de Bona da; Menezes,Cristiano Ragagnin de.
ABSTRACT: Technique of complex coacervation was used to produce microcapsules of Lactobacillus acidophilus La-5 encapsulated in gelatin and gum arabic which were then freeze-drying. Microcapsules were characterized using scanning electron and optical microscopy, and resistance of probiotics was evaluated during release into a simulated gastrointestinal tract and storage at different temperatures. The complex coacervation process produced microcapsules with a high encapsulation efficiency (77.60% and 87.53%), ranging from 127.14-227.05 μm with uniform distribution. Microencapsulation was an efficient approach to achieve significant protection of probiotics against simulated gastrointestinal conditions compared with free cells. Encapsulation also improved...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Microencapsulation; Lactobacillus acidophilus; Gelatin; Gum Arabic.
Ano: 2019 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-84782019000700752
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Production and characterization of alginate microparticles obtained by ionic gelation and electrostatic adsorption of concentrated soy protein Ciência Rural
Silverio,Gabriela Barros; Sakanaka,Lyssa Setsuko; Alvim,Izabela Dutra; Shirai,Marianne Ayumi; Grosso,Carlos Raimundo Ferreira.
ABSTRACT: Microencapsulation is used for protection and release of bioactive compounds. Combination of encapsulation methods allows the production of matrices with better technological properties compared to the application of one of the methods alone. Use of ionic gelation produces porous microparticles, and coating it with a protein, by electrostatic interaction, may contribute to a better protection of the active compound. The objective of the research was to produce alginate microparticles (AG) through ionic gelation and to coat them with soluble protein from soy protein concentrate. Two factors were studied, calcium concentration during ionic gelation (0.8, 1.6 and 2.4% w/w) and pH (3.5 and 7.0) of the protein solution for electrostatic interaction....
Tipo: Info:eu-repo/semantics/article Palavras-chave: Microencapsulation; Ionic gelation; Electrostatic interaction; Alginate; Soy protein.
Ano: 2018 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-84782018001200750
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Microencapsulation of probiotics using sodium alginate Ciência Rural
Etchepare,Mariana de Araújo; Barin,Juliano Smanioto; Cichoski,Alexandre José; Jacob-Lopes,Eduardo; Wagner,Roger; Fries,Leadir Lucy Martins; Menezes,Cristiano Ragagnin de.
The consumption of probiotics is constantly growing due to the numerous benefits conferred on the health of consumers. In this context, Microencapsulation is a technology that favors the viability of probiotic cultures in food products, mainly by the properties of protection against adverse environmental conditions and controlled release. Currently there are different procedures for microencapsulation using polymers of various types of natural and synthetic origin. The use of sodium alginate polymers is one of the largest potential application in the encapsulation of probiotics because of their versatility, biocompatibility and toxicity exemption. The aim of this review is to present viable encapsulation techniques of probiotics with alginate, emphasizing...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Alginate; Controlled release; Microencapsulation; Probiotics..
Ano: 2015 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-84782015000701319
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Cross-linked coacervates of cashew gum and gelatin in the encapsulation of pequi oil Ciência Rural
Alexandre,Joana de Barros; Barroso,Tiago Linhares Cruz Tabosa; Oliveira,Marília de Albuquerque; Mendes,Francisco Rogênio da Silva; Costa,José Maria Correia da; Moreira,Renato de Azevedo; Furtado,Roselayne Ferro.
ABSTRACT: Pequi oil is rich in bioactive compounds which can be encapsulated to increase protection against extrinsic environmental factors. A delayed degradation of pequi oil may occur by using microencapsulation technology, in addition to masking unpleasant flavors and aromas. Complex coacervation is a technique based on the electrostatic interaction between two oppositely charged biopolymers which form a matrix complexed around an agent of interest. However, cross-linking the particles is often necessary in order to make them more rigid. The objective of this research was to produce and characterize pequi oil microparticles in a cashew gum (CG) and gelatin (GE) matrix cross-linked with tannic acid. Cross-linked pequi oil microparticles were produced by...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Microencapsulation; Complex coacervation; Cross-linking; Tannic acid; Encapsulation efficiency.
Ano: 2019 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-84782019001200753
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Encapsulation of Lactobacillus acidophilus and different prebiotic agents by external ionic gelation followed by freeze-drying Ciência Rural
Poletto,Gabriela; Fonseca,Bruna de Souza; Raddatz,Greice Carine; Wagner,Roger; Lopes,Eduardo Jacob; Barin,Juliano Smanioto; Flores,Erico Marlon de Moraes; Menezes,Cristiano Ragagnin de.
ABSTRACT: The aim of this study was to investigate the influence of the addition of prebiotics rice bran, inulin and hi-maize, on the survival of Lactobacillus acidophilus in alginate microparticles obtained by external ionic gelation followed by freeze-drying. The microparticles size ranged from 127.5μm to 234.6μm. Microparticles added from the different prebiotics demonstrated an increase in the protection of the microorganism, which presented greater viability against the gastrointestinal simulation. As for storage under different conditions, rice bran treatment at 25ºC kept probiotics viable for 30 days. Under storage conditions -18°C and 7°C, treatments containing prebiotics hi-maize and rice bran maintained viable probiotic microorganisms for a...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Microencapsulation; Probiotics; Rice bran; Inulin; Hi-maize.
Ano: 2019 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-84782019000200751
Registros recuperados: 25
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