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Abreu,Viviane Gomes da Costa; Silva,Marilda Conceição da; Magalhães,Rozângela Manfrini; Piló-Veloso,Dorila; Xavier,Izelene Felício da Silva; Oliveira,Patrícia Machado; Alcântra,Antônio Flávio de Carvalho. |
Three coumarins, 5-methoxypsoralene, xanthyletin, and (-)-marmesin, have been isolated from the ethanolic extract of the stem of the Amazonian plant Brosimum potabile. The structures were determined on the basis of NMR analyses and by comparison with spectroscopic data in the literature. The analysis of the hexane fractions by GC-MS in EIMS mode suggested the presence of (1-methylpentyl)-benzene; α,α-dimethyl-4-(1-methylethyl)-benzenemethanol; 1-methyl-3,5-bis(1-methylethyl)-benzene; urs-12-ene; chola-5,22-dien-3β-ol; cholesta-4,6-dien-3β-ol; sitosteryl 9(Z)-octadecenoate; cholesta-5,22-dien-3β-ol; cholesta-4,6,22-trien-3-one; and cholesta-4,22-dien-3-one. NMR data of other hexane fractions indicated the presence of 3β-acetoxy-lup-12,20(29)-diene;... |
Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Brosimum potabile; Coumarins; Pentacyclic triterpenes; Structural characterization by NMR and GC/MS. |
Ano: 2010 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0044-59672010000400011 |
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Abreu,Viviane Gomes da Costa; Corrêa,Geone Maia; Lagos,Izandina Aparecida dos Santos; Silva,Roqueline Rodrigues; Alcântara,Antônio F. de C.. |
The ethanol extract from stem bark of Sacoglottis uchi Huber (popularly known as uchi in the Amazon Region) was submitted to chromatographic fractionation. The dichloromethane fractions provided the pentacyclic triterpene 3-oxo-friedelin (1). The dichloromethane:methanol fractions provided the pentacyclic triterpenes pseudotaraxasterol (2), lupeol (3), a-amyrin (4), betulin (5), and methyl 2ß,3ß-dihydroxy-urs-12-en-28-oate (6) and a mixture of the steroids sitosterol (7) and stigmasterol (8). Their chemical structures were determined by NMR spectroscopy and comparison with spectroscopic data from the literature. All compounds are described for the first time in this species. |
Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Humiriaceae; Medicinal plants; Amazon Region; Triterpenes. |
Ano: 2013 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0044-59672013000400015 |
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