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| Masson,José; Cardoso,Maria das Graças; Zacaroni,Lidiany Mendonça; Anjos,Jeancarlo Pereira dos; Sackz,Adelir Aparecida; Machado,Ana Maria de Resende; Nelson,David Lee. |
| Seventy-one samples of sugarcane spirits from small and average size stills produced in the northern and southern Minas Gerais (Brazil) were analyzed for acrolein using HPLC (High Performance Liquid Chromatography). Ethanol and copper concentrations and volatile acidity were also determined according to methods established by the Ministry of Agriculture, Livestock and Supply (MAPA). A total of 9.85% of the samples tested showed levels of acrolein above the legal limits, while the copper concentrations of 21.00% of the samples and the volatile acidity of 8.85% of the samples were higher than the limits established by the Brazilian legislation. The concentration of acrolein varied from 0 to 21.97 mg.100 mL-1 of ethanol. However, no significant difference at... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Contaminants; Congeners; Minas Gerais. |
| Ano: 2012 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0101-20612012000300021 |
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| Menezes,Joyce Castro de; Borges,Gabriela Borba Vilela; Gomes,Fátima de Cássia Oliveira; Vieira,Mariana de Lourdes Almeida; Marques,Andréa Rodrigues; Machado,Ana Maria de Resende. |
| ABSTRACT: The interest in the use of green tea (Camellia sinensis) (L.) Kuntze (Theaceae) products have increased in the last few years due to its medicinal properties. In the present study, we proposed that headspace solid phase microextraction, in combination with gas chromatography coupled to mass spectrometric could be an efficient method to assess the volatile compounds and to ensure the quality control of C. sinensis. We have also compared the anatomical leaf of different commercial green tea samples, analyzed the information in their labels and determined the presence of foreign materials, moisture content, total ashes and microorganisms. Among the 30 analyzed samples, six were identified as C. sinensis according to the anatomical study; 83.4% were... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Green tea; GC-MS; SPME; Quality control. |
| Ano: 2019 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-84782019000300751 |
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