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	Provedor de dados BJPS (1) Autor Kumar,B. V. V. Ravi (1) Panda,Sagar Suman (1) Swain,Suchismita (1) Palavra-chave Glycopyrrolate (1) Life cycle management (1) Liquid chromatography (1) Stability-indicating (1) Validation (1) Tipo do documento Info:eu-repo/semantics/article (1) Ano 2020 (1) País Brazil (1) Idioma Inglês (1)		Ordenar por:  Relevância Autor Título Ano Registros recuperados: 1 Primeira ... 1 ... Última Analytical lifecycle management oriented development and validation of a new stability-indicating ultra-fast liquid chromatographic method: case study of Glycopyrrolate BJPS Panda,Sagar Suman; Kumar,B. V. V. Ravi; Swain,Suchismita. A new stability-indicating liquid chromatographic method was developed and validated for the estimation of glycopyrrolate in pharmaceutical formulations. A contemporary approach to analytical life-cycle management was followed to develop a robust and reliable chromatographic method. Scouted method variables such as % methanol, the strength of tetra butyl ammonium hydrogen sulfate and mobile phase flow rate were optimized using the design of experiment approach and their effect on critical quality attributes was studied. The critical quality attributes viz. retention time, theoretical plate count and symmetry factor were highly influenced by the three critical method variables. Optimum chromatography was attained on a C-18 column with a mobile phase... Tipo: Info:eu-repo/semantics/article Palavras-chave: Glycopyrrolate; Stability-indicating; Liquid chromatography; Life cycle management; Validation. Ano: 2020 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1984-82502020000100605 Registros recuperados: 1 Primeira ... 1 ... Última

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