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MAGALHÃES, S. P.; SILVA, J. M. G. da; GRAÇA, J. P. da; NUNES, E. de O.; ZOCOLO, G. J.; HOFFMANN-CAMPO, C. B.; ZERAIK, M. L.. |
Abstract: This study aimed to establish a method for the extraction, enrichment, and identification of volatile organic compounds (VOCs) released by the flowers of purple (BRS 399) and white (DONMARIO 6563) soybean varieties. We tested the Static Headspace (HS) and Solid Phase Microextraction (SPME) methods using various fibre types: PDMS (Polydimethylsiloxane), PDMS/DVB (Divinylbenzene), and PDMS/DVB/CAR (Carboxen). We employed gas chromatography-mass spectrometry (GC-MS) to identify the VOCs. The SPME method with PDMS/DVB and PDMS/DVB/CAR fibres yielded the highest number of extracted compounds for both soybean cultivars. Notably, 67 compounds were detected in Glycine max. L for the first time. Using the developed method, we were able to detect 52 and 57... |
Tipo: Artigo de periódico |
Palavras-chave: Cromatografia em fase gasosa; Espectrometria de massa; Flores de soja; Microextração; Composto orgânico volátil; Soybean flowers; Gas chromatography; Mass spectrometry; Microextraction; Volatile organic compounds. |
Ano: 2023 |
URL: http://www.alice.cnptia.embrapa.br/alice/handle/doc/1164479 |
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