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One-Single Extraction Procedure for the Simultaneous Determination of a Wide Range of Polar and Nonpolar Organic Contaminants in Seawater ArchiMer
Fauvelle, Vincent; Castro-jimenez, Javier; Schmidt, Natascha; Carlez, Benoit; Panagiotopoulos, Christos; Sempere, Richard.
A rapid analytical method including one-single solid-phase extraction (SPE) procedure followed by gas and liquid chromatography coupled with high resolution mass spectrometry detection (GC-MS and LC-HRMS respectively) was developed for the quantification of 40 organic compounds (1.6 < log K-ow < 9.5) in seawater including both legacy and emerging contaminants, with a focus on the most common plastic organic additives. This new method allowed for the analyses of nine organophosphate esters (OPEs), seven phthalates (PAEs), six bisphenols (BPs), five perfluorinated compounds (PFCs), and thirteen legacy organochlorinated compounds (OCs, including polychlorobiphenyles and pesticides) with recoveries in the ranges of 57-124% for OPEs, 52-163% for PAEs,...
Tipo: Text Palavras-chave: Plastic additive; Seawater; Organic contaminants; Legacy contaminants; Phtalates; Bisphenol; Organophosphate esters.
Ano: 2018 URL: https://archimer.ifremer.fr/doc/00645/75716/76697.pdf
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