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| Mattio, Elodie; Ollivier, Nadia; Robert-peillard, Fabien; Di Rocco, Robert; Branger, Catherine; Margaillan, Andre; Brach-papa, Christophe; Knoery, Joel; Bonne, Damien; Boudenne, Jean-luc; Coulomb, Bruno. |
| 3D printing technology is increasingly used in flow analysis, to develop low cost and tailor-made devices. The possibility of grafting specific molecules onto 3D printed parts offers new perspectives for the development of flow systems. In this study, a MPFS system including a dicarboxylate 1,5-diphenyl-3-thiocarbazone grafted 3D-printed device has been developed for mercury determination. For this purpose, the surface of 3D-printed cuboids was first modified with amine functional groups and then grafted with dicarboxylate 1,5-diphenyl-3-thiocarbazone. This new grafted device resulted in selective mercury preconcentration with extraction and elution yields higher than 90% even at high sampling flow rates. The detection can then be carried out in two ways:... |
| Tipo: Text |
Palavras-chave: Stereolithography Poly(methylmethacrylate) grafting Dicarboxylate 1; 5-diphenyl-3-thiocarbazone Multi pumping flow system Mercury. |
| Ano: 2019 |
URL: https://archimer.ifremer.fr/doc/00505/61682/65631.pdf |
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| Mattio, Elodie; Robert-peillard, Fabien; Vassalo, Laurent; Branger, Catherine; Margaillan, Andre; Brach-papa, Christophe; Knoery, Joel; Boudenne, Jean-luc; Coulomb, Bruno. |
| In recent years, the development of 3D printing in flow analysis has allowed the creation of new systems with various applications. Up to now, 3D printing was mainly used for the manufacture of small units such as flow detection cells, preconcentration units or mixing systems. In the present study, a new 3D printed lab-on-valve system was developed to selectively quantify lead and cadmium in water. Different technologies were compared for lab-on-valve 3D printing. Printed test units have shown that stereolithography or digital light processing are satisfactory techniques for creating complex lab-on-valve units. The lab-on-valve system was composed of two columns, eight peripheral ports and a central port, and a coil integrating baffles to increase mixing... |
| Tipo: Text |
Palavras-chave: Stereolithography; Digital light processing; LOV-MSFIA; Natural waters. |
| Ano: 2018 |
URL: https://archimer.ifremer.fr/doc/00427/53874/54932.pdf |
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| Mattio, Elodie; Robert-peillard, Fabien; Branger, Catherine; Puzio, Kinga; Margaillan, Andre; Brach-papa, Christophe; Knoery, Joel; Boudenne, Jean-luc; Coulomb, Bruno. |
| The development of 3D printing in recent years opens up a vast array of possibilities in the field of flow analysis. In the present study, a new 3D-printed flow system has been developed for the selective spectrophotometric determination of lead in natural waters. This system was composed of three 3D-printed units (sample treatment, mixing coil and detection) that might have been assembled without any tubing to form a complete flow system. Lead was determined in a two-step procedure. A preconcentration of lead was first carried out on TrisKem Pb Resin located in a 3D-printed column reservoir closed by a tapped screw. This resin showed a high extraction selectivity for lead over many tested potential interfering metals. In a second step, lead was eluted by... |
| Tipo: Text |
Palavras-chave: Lead determination; 3D-printed MPFS system; Stereolithography; Natural waters. |
| Ano: 2017 |
URL: https://archimer.ifremer.fr/doc/00377/48770/49290.pdf |
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