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Registros recuperados: 7
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Do Aggregate Size Classes of the Subsurface Soil Horizon Have Different Chemical/Mineralogical Properties? Rev. Bras. Ciênc. Solo
Mitton,Rolff Vladimir; Melo,Vander Freitas; Pauletti,Volnei.
ABSTRACT Variations in chemical and mineralogical properties of a soil can occur at short vertical and horizontal distances. The objective of the present study was to evaluate the chemical and mineralogical soil properties of different aggregate classes from young (Ustrochrept) and highly weathered (Acrustox) soils from the state of Paraná, Brazil. Undisturbed blocks (0.20 ×0.20 ×0.20 m) of soils were separated into aggregate classes: Acrustox – 8.0-4.0 mm; 4-2 mm; 2.0-0.5 mm; 0.5-0.2 mm; and <0.2 mm; and Ustrochrept – 8.0-4.0 mm; 4.0-2.0 mm; 2.0-0.5 mm; and 0.5-0.2 mm. The exchangeable K contents showed an opposite behavior for the two soils: higher contents in the Acrustox for the larger aggregate classes and higher contents in the Ustrochrept for the...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Kaolinite; Hematite; Goethite; Gibbsite; K reserve.
Ano: 2019 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-06832019000100401
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Microwave Acid Extraction to Analyze K and Mg Reserves in the Clay Fraction of Soils Rev. Bras. Ciênc. Solo
Batista,Araína Hulmann; Melo,Vander Freitas; Gilkes,Robert.
ABSTRACT: Extraction of K and Mg with boiling 1 mol L-1 HNO3 in an open system for predicting K and Mg uptake by plants is a method of low reproducibility. The aim of this study was to compare the extraction capacity of different acid methods relative to hydrofluoric acid extraction for K and Mg. A further objective was to develop a chemical extraction method using a closed system (microwave) for nonexchangeable and structural forms of these nutrients in order to replace the traditional method of extraction with boiling HNO3 on a hot plate (open system). The EPA 3051A method can be used to estimate the total content of K in the clay fraction of soils developed from carbonate and phyllite/mica schist rocks. In the clay fraction of soils developed from...
Tipo: Info:eu-repo/semantics/article Palavras-chave: EPA 3051A; EPA 3052; Aqua regia; Boiling nitric acid; Microwave extraction; Nonexchangeable K.
Ano: 2016 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-06832016000100431
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Pedogenic Iron Oxides in Iron-Rich Oxisols Developed from Mafic Rocks Rev. Bras. Ciênc. Solo
Camêlo,Danilo de Lima; Ker,João Carlos; Fontes,Maurício Paulo Ferreira; Corrêa,Marcelo Metri; Costa,Antonio Carlos Saraiva da; Melo,Vander Freitas.
ABSTRACT Despite the considerable amount of information on the mineralogical characteristics of pedogenic Fe oxides in Brazilian soils, there are few studies on Fe-rich soils developed from mafic rocks with taxonomic identities at lower categorical levels. This study evaluated the mineralogical characteristics of pedogenic Fe oxides in B horizons (Bw) of Fe-rich Oxisols developed from several mafic rocks in the state of Minas Gerais, Brazil. The Bw horizons were sampled at a 0.8-1.0 m depth in 13 Ferric and Perferric Rhodic Oxisols along with a Mesoferric Typic Oxisol originating from basalt, gabbro, tuffite, amphibolite and itabirite in Minas Gerais. The selected soils have taxonomic identities up to the fourth categorical level of the Brazilian System of...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Hematite; Maghemite; Crystallographic characteristics; Al-substitution; Selective dissolution.
Ano: 2017 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-06832017000100413
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Validation of a Standard Operating Procedure (SOP) for Forensic Soils Investigation in Brazil Rev. Bras. Ciênc. Solo
Testoni,Samara Alves; Melo,Vander Freitas; Dawson,Lorna Anne; Salvador,Fábio Augusto da Silva; Kunii,Paulo Akira.
ABSTRACT Soil traces are useful as forensic evidence due to their potential to transfer and adhere to different types of surfaces on a range of objects or persons. Several works have been developed in forensic soils, under different analytical approaches. However, in Brazil, only the researches from the Group of the Federal University of Paraná have developed works with soils under a forensic approach. Focus has been given on the sequential chemical analyses and mineralogical techniques once they presented a large potential to discriminate soil samples, even that originated from the same bedrock. In this way, this work aimed to test a Standard Operating Procedure (SOP) for forensic soil sampling and an analytical protocol in Brazil between the academy and...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Forensic science; Soil evidence; Sequential chemical analysis; Gibbsite; Iron oxides.
Ano: 2019 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-06832019000100410
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Land Use and Changes in Soil Morphology and Physical-Chemical Properties in Southern Amazon Rev. Bras. Ciênc. Solo
Melo,Vander Freitas; Orrutéa,Alessandro Góis; Motta,Antônio Carlos Vargas; Testoni,Samara Alves.
ABSTRACT Many Amazonian farmers use the slash-and-burn method rather than fertilization for crop production. The aim of the present study was to evaluate changes in the morphological, physical, and chemical properties of naturally fertile Inceptisols after conversion from native forest to different uses in southern Amazonia, Brazil. Land covered by dense native forest (NF) was split into four areas of 1.0 ha each. Three areas were slashed and burned and then cultivated for 11 years with coffee (CO), secondary forest (SF), and pasture (PA). Four soil profiles were sampled in each treatment (four uses × four replicates). The mean value distribution of each physical and chemical analysis was determined for different depths, and standard error bars were placed...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Secondary forest; Coffee; Pasture; Slash and burn; Ash effect.
Ano: 2017 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-06832017000100523
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Identification of Heavy Metals in Crystals of Sand and Silt Fractions of Soils by Scanning Electron Microscopy (SEM EDS/WD-EPMA) Rev. Bras. Ciênc. Solo
Batista,Araína Hulmnn; Melo,Vander Freitas; Gilkes,Robert; Roberts,Malcolm.
ABSTRACT Studies of heavy metals are concentrate on clay fractions, but coarser fractions of the soil can constitute significant sources of structural forms of heavy metals. The aim of this study was to evaluate the occurrence of heavy metals in the structure of minerals of the sand and silt fractions of soils from three different parent materials (metamorphic rocks and granite) in southern Brazil using SEM/EDS - Scanning Electron Microscopy with Energy Dispersive Spectroscopy and with WD-EPMA - with Wavelength Dispersive-Electron Probe Microanalysis. We sampled soils from two areas naturally rich in heavy metals, with high mineral deposits (galena - PbS) hosted in carbonate rocks and phyllite/mica schist. The main form of Ba in the sand and silt fractions...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Plumbogummite; Barite; Isomorphic substitution; Polished sample.
Ano: 2018 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-06832018000100408
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Do Aqua Regia and EPA 3051A methods underestimate the pseudo-total P content in clay soil fraction? Ciência e Agrotecnologia
Melo,Vander Freitas; Guedes,Lauriane Guidolin.
ABSTRACT It is common the use of 3051A and aqua regia methods to assess the pseudo-total and total P contents in soil and in its fractions. However, previous study has shown the formation of large amounts of short-range order materials (SRO) in the residues of these extractions. The objective of this work was to evaluate whether phosphate resorb in the SRO formed in the residue of 3051A and aqua regia extractions in clay soil fraction. Residues obtained from the 3051A and aqua regia were recovered from filter papers. To characterize the SRO in these residues, sequential extractions were performed with 0.2 mol L-1 ammonium oxalate and 0.5 mol L-1 NaOH. The maximum pseudo-total P content extracted by aqua regia was 6800 mg kg-1. If SRO formed during this...
Tipo: Info:eu-repo/semantics/article Palavras-chave: Short-range order materials; Inner sphere adsorption; Isomorphic substitution; Sequential extractions.
Ano: 2020 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1413-70542020000100234
Registros recuperados: 7
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