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Determination of methanol residues in crude glycerol for animal feed by gas chromatography Scientia Agricola
Nazato,Carina; Romero,Alessandra de Cássia; Abdalla,Adibe Luiz.
ABSTRACT: Crude glycerol is a major by-product of biodiesel production and is an economical additive feed for ruminants. However, residual methanol in crude glycerol can be harmful to animal health. Several methods exist for quantifying methanol residues in biodiesel, yet few have been described that identify the methanol level in crude glycerol. We propose a method for determining the methanol level in crude glycerol destined for animal feed. Crude glycerol was extracted from the headspace and quantified by gas chromatography using a flame ionization detector (GC-FID). The method was linear up to 0.5 % of methanol. The limits of detection (LOD) and quantification (LOQ) were 0.015 and 0.031 %, respectively. No significant matrix effects were observed....
Tipo: Info:eu-repo/semantics/article Palavras-chave: Co-product; Feedstuff; Biodiesel; Toxic compound; Ruminant.
Ano: 2019 URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-90162019001600527
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