|
|
| Santos,Éder José dos; Santos,Arlene Bispo dos; Herrmann,Amanda Beatriz; Kulik,Suzete; Baika,Loana Mara; Tormen,Luciano; Curtius,Adilson José. |
| An on-line method for Cd and Pb pre-concentration and simultaneous determination in acid digested seafood by inductively coupled plasma optical emission spectrometry (ICP OES) was developed. The on-line pre-concentration was based on the complex formation of the analytes with the ammonium salt of O,O-diethyldithiophosphate (DDTP) and using the Amberlite XAD-4 resin as a solid support in a homemade column. Different conditions of the flow injection system, such as solutions flow rates, nebulizer pressure and eluent concentration were optimized. Three certified reference materials of lobster hepatopancreas, dogfish liver and fish protein, three samples of fish muscle and three samples of shrimp were digested with HNO3, H2O2 and H2SO4 in a microwave system... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Cd; Pb; ICP OES; Diethyldithiophosphate; XAD-4; Seafood; Solid phase extraction. |
| Ano: 2013 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-89132013000100017 |
| |
