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| BARROS,JOÉLIA M.; BEZERRA,MARCOS A.; VALASQUES,GISSELI S.; NASCIMENTO JÚNIOR,BARAQUÍZIO B. DO; SOUZA,ANDERSON S.; ARAGÃO,NÁDIA M. DE. |
| In this work, multivariate optimization techniques were used to develop a method based on the ultrasound-assisted extraction for copper, manganese, nickel and zinc determination from rations for chicken nutrition using flame atomic absorption spectrometry. The proportions of extracting components (2.0 mol.L–1 nitric, hydrochloric and acetic acid solutions) were optimized using centroid-simplex mixture design. The optimum proportions of this mixture taken as percentage of each component were respectively 20%, 37% and 43%. Variables of method (sample mass, sonication time and final acid concentration) were optimized using Doehlert design. The optimum values found for these variables were respectively 0.24 g, 18s and 3.6 mol.L–1. The developed method allows... |
| Tipo: Info:eu-repo/semantics/article |
Palavras-chave: Rations to chicken; Ultrasound-assisted extraction; Mixture design; Doehlert design; Metals. |
| Ano: 2013 |
URL: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0001-37652013000300891 |
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